Structures published

Total: 223

Compound 5

C₁₁H₉F₄NO₂Sn

Savjani, Nicky Lancaster, Simon J.Bew, Sean Hughes, David L.Bochmann, Manfred

Dalton transactions (Cambridge, England : 2003) (2011) 40, 5 1079-1090

a=19.1926(6)Å b=6.6264(2)Å c=20.1512(7)Å

α=90.00° β=90.257(3)° γ=90.00°

Compound 7

C₈F₄INO_2,C₂H₃N

Savjani, Nicky Lancaster, Simon J.Bew, Sean Hughes, David L.Bochmann, Manfred

Dalton transactions (Cambridge, England : 2003) (2011) 40, 5 1079-1090

a=9.4073(7)Å b=6.3030(5)Å c=10.1518(10)Å

α=90.00° β=108.929(9)° γ=90.00°

Compound 8a

C₂₆H₁₅AuF₄NO₂P

Savjani, Nicky Lancaster, Simon J.Bew, Sean Hughes, David L.Bochmann, Manfred

Dalton transactions (Cambridge, England : 2003) (2011) 40, 5 1079-1090

a=13.79281(11)Å b=12.00838(11)Å c=28.1090(3)Å

α=90.00° β=100.4139(10)° γ=90.00°

Compound 9

C₁₂H₈AuF₄NO₂S_,C₇H₈

Savjani, Nicky Lancaster, Simon J.Bew, Sean Hughes, David L.Bochmann, Manfred

Dalton transactions (Cambridge, England : 2003) (2011) 40, 5 1079-1090

a=11.8670(17)Å b=23.7634(14)Å c=6.6297(5)Å

α=90.00° β=90.071(9)° γ=90.00°

Compound 10

C₂₀H₆AgAuF₈N₄O_4,C₂H₃N

Savjani, Nicky Lancaster, Simon J.Bew, Sean Hughes, David L.Bochmann, Manfred

Dalton transactions (Cambridge, England : 2003) (2011) 40, 5 1079-1090

a=8.24928(9)Å b=9.49150(15)Å c=16.8812(3)Å

α=94.1577(13)° β=94.4125(11)° γ=111.3597(12)°

Compound 8b

C₂₆H₃₃AuF₄NO₂P_,0.5(C₇H₈)

Savjani, Nicky Lancaster, Simon J.Bew, Sean Hughes, David L.Bochmann, Manfred

Dalton transactions (Cambridge, England : 2003) (2011) 40, 5 1079-1090

a=11.3527(8)Å b=11.7282(9)Å c=11.9341(9)Å

α=74.895(6)° β=69.615(7)° γ=72.833(6)°

Compound 11

C₃₆H₃₀AuP_2,C₄₄B₂F₃₄NO_2,ca_1.5(C₄H₈O)

Savjani, Nicky Lancaster, Simon J.Bew, Sean Hughes, David L.Bochmann, Manfred

Dalton transactions (Cambridge, England : 2003) (2011) 40, 5 1079-1090

a=15.4133(11)Å b=32.505(2)Å c=16.4236(12)Å

α=90.00° β=89.997(2)° γ=90.00°

C₂₁H₈F₁₈N₂

Carrera, Nora Savjani, Nicky Simpson, Jason Hughes, David L.Bochmann, Manfred

Dalton transactions (Cambridge, England : 2003) (2011) 40, 5 1016-1019

a=18.0973(13)Å b=7.9809(5)Å c=15.6913(10)Å

α=90.00° β=92.109(6)° γ=90.00°

C₃₉H₂₂AuF₁₈N₂P

Carrera, Nora Savjani, Nicky Simpson, Jason Hughes, David L.Bochmann, Manfred

Dalton transactions (Cambridge, England : 2003) (2011) 40, 5 1016-1019

a=19.7418(5)Å b=16.0248(4)Å c=25.9858(9)Å

α=90.00° β=111.892(3)° γ=90.00°

C₅₇H₃₇F₁₈N₂P₂CU_,C_4.4

Carrera, Nora Savjani, Nicky Simpson, Jason Hughes, David L.Bochmann, Manfred

Dalton transactions (Cambridge, England : 2003) (2011) 40, 5 1016-1019

a=19.2547(5)Å b=20.3882(5)Å c=14.5824(4)Å

α=90.00° β=100.886(2)° γ=90.00°

C₂₆H₂₈Zr

Bochmann, Manfred Green, Malcolm L. H.Powell, Annie K.Saßmannshausen, Jörg Triller, Michael U.Wocadlo, Sigrid

Journal of the Chemical Society, Dalton Transactions (1999) 1 43

a=9.857(2)Å b=13.365(3)Å c=8.244(2)Å

α=103.48(2)° β=101.19(2)° γ=87.95(2)°

C₄₆H₄₈BF₁₅HfOSi₂

Pindado, Gerardo Jiménez Thornton-Pett, Mark Hursthouse, Michael B.Coles, Simon J.Bochmann, M.

Journal of the Chemical Society, Dalton Transactions (1999) 10 1663

a=11.1910(15)Å b=13.1465(15)Å c=17.506(2)Å

α=104.763(10)° β=94.315(11)° γ=103.276(10)°

C₃₄H₂₈BF₁₅Si₂Zr

Pindado, Gerardo Jiménez Thornton-Pett, Mark Hursthouse, Michael B.Coles, Simon J.Bochmann, M.

Journal of the Chemical Society, Dalton Transactions (1999) 10 1663

a=10.068(7)Å b=11.442(16)Å c=16.218(17)Å

α=96.79(3)° β=105.19(5)° γ=94.15(6)°

C₃₄H₄₅Cl₇N₂P₂Si₂Ti

Sarsfield, Mark J.Thornton-Pett, Mark Bochmann, Manfred

Journal of the Chemical Society, Dalton Transactions (1999) 19 3329

a=22.4593(7)Å b=9.4978(3)Å c=21.4978(6)Å

α=90.00° β=113.0940(14)° γ=90.00°

C₂₅H₂₈AuNO_,H₂O

Dragos-Adrian Rosca Dan A. Smith Manfred Bochmann

Chem.Commun. (2012) 48, 7247

a=14.9668(4)Å b=11.3514(3)Å c=12.9152(4)Å

α=90.00° β=99.366(3)° γ=90.00°

Compound 3a

C₁₇H₁₆NOP

Broomfield, Lewis M.Wright, Joseph A.Bochmann, Manfred

Dalton Transactions (2009) 39 8269-8279

a=11.3992(3)Å b=5.75940(10)Å c=22.1848(5)Å

α=90.00° β=95.068(1)° γ=90.00°

Compound 5a

C₃₈H₄₂N₄O₂P₂Ti

Broomfield, Lewis M.Wright, Joseph A.Bochmann, Manfred

Dalton Transactions (2009) 39 8269-8279

a=15.392(5)Å b=12.636(5)Å c=18.352(5)Å

α=90.00° β=90.00° γ=90.00°

Compound 5c

C₄₆H₅₈N₄O₂P₂Ti_,2.5(C₆H₆)

Broomfield, Lewis M.Wright, Joseph A.Bochmann, Manfred

Dalton Transactions (2009) 39 8269-8279

a=12.1366(13)Å b=16.2331(17)Å c=16.3753(17)Å

α=108.236(9)° β=95.852(9)° γ=107.144(9)°

Compound 7b

C₄₂H₄₆N₂O₂P₂Zn_,C₇H₈

Broomfield, Lewis M.Wright, Joseph A.Bochmann, Manfred

Dalton Transactions (2009) 39 8269-8279

a=11.2743(8)Å b=11.3563(8)Å c=18.7268(13)Å

α=81.072(6)° β=75.302(6)° γ=74.362(6)°

Compound 8a

C₅₁H₄₅N₃O₃P₃Y_,C₇H₈

Broomfield, Lewis M.Wright, Joseph A.Bochmann, Manfred

Dalton Transactions (2009) 39 8269-8279

a=14.899(3)Å b=18.890(3)Å c=22.165(3)Å

α=90.00° β=127.768(10)° γ=90.00°

Tris[3,6-di-tert-butyl-1-(isoquinolin-1-yl)naphthalen-2-olato- κ^2^N,O]aluminium(III) toluene sesquisolvate

C₈₁H₈₄AlN₃O_3,1.5(C₇H₈)

Broomfield, Lewis M.Bochmann, Manfred Wright, Joseph A.

Acta Crystallographica Section C (2012) 68, 8 m226-m228

a=13.0728(2)Å b=15.9452(3)Å c=19.4565(4)Å

α=75.2170(10)° β=75.2620(10)° γ=74.2000(10)°

Compound (VI)

C₁₇H₁₆Cl₄NPTi

Broomfield, Lewis M.Bochmann, Manfred Wright, Joseph A.

Acta Crystallographica Section C (2010) 66, 3 m79-m82

a=8.1481(17)Å b=8.6323(16)Å c=14.202(3)Å

α=98.159(15)° β=98.727(16)° γ=100.588(16)°

Compound (V)

0.43(C₁₇H₁₆NOP)_,0.57(C₁₇H₁₆NP)

Broomfield, Lewis M.Bochmann, Manfred Wright, Joseph A.

Acta Crystallographica Section C (2010) 66, 3 m79-m82

a=9.6282(9)Å b=15.2848(14)Å c=20.391(2)Å

α=90.00° β=101.376(8)° γ=90.00°

1-[2-(2,6-Diisopropylanilino)-1-naphthyl]isoquinoline

C₃₁H₃₀N₂

Howard, Ruth H.Theobald, Nicola Bochmann, Manfred Wright, Joseph A.

Acta Crystallographica Section C (2010) 66, 6 o310-o312

a=9.0996(10)Å b=11.2154(12)Å c=23.974(3)Å

α=90.00° β=90.00° γ=90.00°

Compound (II)

C₃₄H₅₄N₂O₂Zn

Howard, Ruth H.Bochmann, Manfred Wright, Joseph A.

Acta Crystallographica Section C (2006) 62, 7 m293-m296

a=12.9275(12)Å b=14.0002(13)Å c=19.6729(14)Å

α=100.747(7)° β=102.467(7)° γ=96.879(8)°

Compound (III)

C₃₂H₅₀N₂O₃Zn

Howard, Ruth H.Bochmann, Manfred Wright, Joseph A.

Acta Crystallographica Section C (2006) 62, 7 m293-m296

a=13.669(3)Å b=17.476(4)Å c=12.989(4)Å

α=90.00° β=93.14(2)° γ=90.00°

C₂₈H₄₁ClCuN

Chotard, Florian Sivchik, Vasily Linnolahti, Mikko Bochmann, Manfred Romanov, Alexander S.

Chemistry of Materials (2020)

a=11.6940(2)Å b=10.3459(2)Å c=20.8452(4)Å

α=90° β=90.626(2)° γ=90°

C₄₀H₄₉AuN_2,2(CH₂Cl₂)

Chotard, Florian Sivchik, Vasily Linnolahti, Mikko Bochmann, Manfred Romanov, Alexander S.

Chemistry of Materials (2020)

a=10.5956(6)Å b=16.5409(6)Å c=12.0346(11)Å

α=90° β=110.128(8)° γ=90°

C₂₄H₃₇ClCuN

Chotard, Florian Sivchik, Vasily Linnolahti, Mikko Bochmann, Manfred Romanov, Alexander S.

Chemistry of Materials (2020)

a=9.9277(7)Å b=10.1798(5)Å c=23.3955(14)Å

α=90° β=96.004(6)° γ=90°

C₄₀H₄₉CuN_2,CH₂Cl₂

Chotard, Florian Sivchik, Vasily Linnolahti, Mikko Bochmann, Manfred Romanov, Alexander S.

Chemistry of Materials (2020)

a=18.4735(4)Å b=10.1510(2)Å c=19.3448(4)Å

α=90° β=90° γ=90°

C₂₈H₄₁AgClN

Chotard, Florian Sivchik, Vasily Linnolahti, Mikko Bochmann, Manfred Romanov, Alexander S.

Chemistry of Materials (2020)

a=10.0759(2)Å b=11.7337(2)Å c=21.2836(3)Å

α=90° β=90.1400(10)° γ=90°

C₃₆H₄₅AgN₂

Chotard, Florian Sivchik, Vasily Linnolahti, Mikko Bochmann, Manfred Romanov, Alexander S.

Chemistry of Materials (2020)

a=30.8829(5)Å b=13.4632(2)Å c=17.0861(3)Å

α=90° β=103.783(2)° γ=90°

C₃₆H₄₅CuN₂

Chotard, Florian Sivchik, Vasily Linnolahti, Mikko Bochmann, Manfred Romanov, Alexander S.

Chemistry of Materials (2020)

a=31.1356(13)Å b=13.3923(5)Å c=16.9072(7)Å

α=90° β=102.687(4)° γ=90°

C₃₆H₄₅AuN₂

Chotard, Florian Sivchik, Vasily Linnolahti, Mikko Bochmann, Manfred Romanov, Alexander S.

Chemistry of Materials (2020)

a=31.0559(6)Å b=13.3859(2)Å c=16.9937(3)Å

α=90° β=103.148(2)° γ=90°

C₂₄H_35.5AuO_0.25P

Rocchigiani, Luca Fernandez-Cestau, Julio Chambrier, Isabelle Hrobárik, Peter Bochmann, Manfred

Journal of the American Chemical Society (2018) 140, 26 8287-8302

a=17.39390(10)Å b=25.81310(10)Å c=21.81150(10)Å

α=90° β=91.63° γ=90°

C₂₉H₄₀AuO₄P

Rocchigiani, Luca Fernandez-Cestau, Julio Chambrier, Isabelle Hrobárik, Peter Bochmann, Manfred

Journal of the American Chemical Society (2018) 140, 26 8287-8302

a=10.30570(10)Å b=14.22560(10)Å c=19.7173(2)Å

α=90° β=90° γ=90°

C₄₈H₆₇AuF₅NO₄

Rocchigiani, Luca Fernandez-Cestau, Julio Chambrier, Isabelle Hrobárik, Peter Bochmann, Manfred

Journal of the American Chemical Society (2018) 140, 26 8287-8302

a=20.9189(2)Å b=17.0445(2)Å c=26.4122(3)Å

α=90° β=90° γ=90°

C₂₆H₄₂Au₂P₂

Rocchigiani, Luca Fernandez-Cestau, Julio Chambrier, Isabelle Hrobárik, Peter Bochmann, Manfred

Journal of the American Chemical Society (2018) 140, 26 8287-8302

a=10.46740(10)Å b=11.89220(10)Å c=22.9414(3)Å

α=90° β=100.8330(10)° γ=90°

(C₁₃H₂₃O₂Y)n

Sanchez-Barba, L. F.Hughes, D. L.Humphrey, S. M.Bochmann, M.

Organometallics (2005) 24, 15 3792-3799

a=14.0919(5)Å b=7.7544(3)Å c=13.6632(6)Å

α=90.00° β=112.552(2)° γ=90.00°

(C₁₃H₂₃O₂Sm)n

Sanchez-Barba, L. F.Hughes, D. L.Humphrey, S. M.Bochmann, M.

Organometallics (2005) 24, 15 3792-3799

a=14.1965(3)Å b=7.8233(2)Å c=13.6478(4)Å

α=90.00° β=111.5527(10)° γ=90.00°

C₃₅H₅₁N₂Sm

Sanchez-Barba, L. F.Hughes, D. L.Humphrey, S. M.Bochmann, M.

Organometallics (2005) 24, 15 3792-3799

a=10.9089(3)Å b=12.3956(3)Å c=13.9731(4)Å

α=65.0710(18)° β=78.7228(14)° γ=73.3055(12)°

C₁₈H₄₂NiSi₄

Schormann, Mark Garratt, Shaun Bochmann, Manfred

Organometallics (2005) 24, 7 1718-1724

a=16.578(3)Å b=12.430(3)Å c=12.698(3)Å

α=90.00° β=90.84(3)° γ=90.00°

C₁₅H₃₉Si₂Sn_2,Hf₂Cl₉

Schormann, Mark Garratt, Shaun Bochmann, Manfred

Organometallics (2005) 24, 7 1718-1724

a=14.860(1)Å b=12.280(1)Å c=19.901(2)Å

α=90.00° β=90.00° γ=90.00°

C₁₅H₃₆Cl₃N₂Si₂Ta

Schormann, Mark Garratt, Shaun Bochmann, Manfred

Organometallics (2005) 24, 7 1718-1724

a=18.928(4)Å b=9.059(2)Å c=14.410(3)Å

α=90.00° β=100.39(3)° γ=90.00°

C₁₈H₄₂CoSi₄

Schormann, Mark Garratt, Shaun Bochmann, Manfred

Organometallics (2005) 24, 7 1718-1724

a=12.323(3)Å b=10.322(2)Å c=21.059(4)Å

α=90.00° β=99.59(3)° γ=90.00°

C₁₅H₃₉Si₂Sn_2,Zr₂Cl₉

Schormann, Mark Garratt, Shaun Bochmann, Manfred

Organometallics (2005) 24, 7 1718-1724

a=14.899(1)Å b=12.310(1)Å c=19.894(1)Å

α=90.00° β=90.00° γ=90.00°

C₁₆H₄₀LiO₄;C₂₈H₆₀Si₆Sm

Woodman, Timothy J.Schormann, Mark Bochmann, Manfred

Organometallics (2003) 22, 14 2938-2943

a=12.511(3)Å b=12.243(2)Å c=19.609(4)Å

α=90.00° β=95.79(3)° γ=90.00°

C₃₂H₆₈KLaOSi₆;C₂H₄O_0.5

Woodman, Timothy J.Schormann, Mark Bochmann, Manfred

Organometallics (2003) 22, 14 2938-2943

a=9.873(2)Å b=12.970(3)Å c=19.496(4)Å

α=76.66(3)° β=77.94(3)° γ=88.78(3)°

C₂H₅ClZn

Guerrero, Antonio Hughes, David L.Bochmann, Manfred

Organometallics (2006) 25, 6 1525-1527

a=6.3802(6)Å b=5.9324(4)Å c=21.8428(17)Å

α=90.00° β=90.00° γ=90.00°

Compound 4b

C₂₁H₂₄Tl_,C₃₆H₂B₂F₃₀N

Yann Sarazin David L. Hughes Nikolas Kaltsoyannis Joseph A. Wright Manfred Bochmann

Journal of the American Chemical Society (2007) 129, 881-894

a=13.781Å b=18.151Å c=21.698Å

α=90.00° β=91.68° γ=90.00°

Compound 2b

C₁₆H₄₀O₄Tl_,C₃₆H₂B₂F₃₀N

Yann Sarazin David L. Hughes Nikolas Kaltsoyannis Joseph A. Wright Manfred Bochmann

Journal of the American Chemical Society (2007) 129, 881-894

a=12.2481(4)Å b=13.7603(5)Å c=17.3040(6)Å

α=86.556(2)° β=76.904(2)° γ=87.120(2)°

Compound 2b

C₁₆H₄₀O₄Tl_,C₃₆H₂B₂F₃₀N

Yann Sarazin David L. Hughes Nikolas Kaltsoyannis Joseph A. Wright Manfred Bochmann

Journal of the American Chemical Society (2007) 129, 881-894

a=12.2481(4)Å b=13.7603(5)Å c=17.3040(6)Å

α=86.556(2)° β=76.904(2)° γ=87.120(2)°

Compound 4b

C₂₁H₂₄Tl_,C₃₆H₂B₂F₃₀N

Yann Sarazin David L. Hughes Nikolas Kaltsoyannis Joseph A. Wright Manfred Bochmann

Journal of the American Chemical Society (2007) 129, 881-894

a=13.781(5)Å b=18.151(8)Å c=21.698(14)Å

α=90.00° β=91.68(5)° γ=90.00°

Compound 3

H₂O₂Tl_4,2(C₃₆H₂B₂F₃₀N)_,4(CH₂Cl₂)

Yann Sarazin David L. Hughes Nikolas Kaltsoyannis Joseph A. Wright Manfred Bochmann

Journal of the American Chemical Society (2007) 129, 881-894

a=11.4827(11)Å b=14.1996(12)Å c=14.2725(8)Å

α=105.075(5)° β=92.968(6)° γ=101.382(7)°

Compound 11b

C₁₂H₂₄O₆Tl_,C₃₆H₂B₂F₃₀N_,2(CH₂Cl₂)

Yann Sarazin David L. Hughes Nikolas Kaltsoyannis Joseph A. Wright Manfred Bochmann

Journal of the American Chemical Society (2007) 129, 881-894

a=12.4566(3)Å b=15.7031(6)Å c=16.4745(10)Å

α=73.710(4)° β=87.071(4)° γ=72.249(3)°

Compound 5b

C₂₄H₃₆Tl_,C₃₆H₂B₂F₃₀N_,2.5(CH₂Cl₂)

Yann Sarazin David L. Hughes Nikolas Kaltsoyannis Joseph A. Wright Manfred Bochmann

Journal of the American Chemical Society (2007) 129, 881-894

a=12.2427(5)Å b=13.9012(4)Å c=19.1784(6)Å

α=84.244(2)° β=86.754(3)° γ=87.660(3)°

C₁₀H₁₅Sn_,C₃₆H₂B₂F₃₀N_,1.5(CH₂Cl₂)

Yann Sarazin David L. Hughes Nikolas Kaltsoyannis Joseph A. Wright Manfred Bochmann

Journal of the American Chemical Society (2007) 129, 881-894

a=28.3882(13)Å b=14.5749(5)Å c=24.8491(14)Å

α=90.00° β=105.688(4)° γ=90.00°

Complex 5e

C₂₁H₂₁Cl₃F₅NO₂Ti

Pennington, Dale A.Clegg, William Coles, Simon J.Harrington, Ross W.Hursthouse, Michael B.Hughes, David L.Light, Mark E.Schormann, Mark Bochmann, Manfred Lancaster, Simon J.

Dalton transactions (Cambridge, England : 2003) (2005) 3 561-571

a=7.2176(2)Å b=34.4138(9)Å c=9.3904(2)Å

α=90.00° β=96.5740(10)° γ=90.00°

C₃₈H₆₆N₄O₂P₂Ti

Broomfield, Lewis M.Wright, Joseph A.Bochmann, Manfred

Dalton Transactions (2009) 39 8269-8279

a=10.7254(5)Å b=19.2509(7)Å c=19.6142(8)Å

α=81.173(3)° β=88.666(2)° γ=89.788(3)°

C₄₀H₅₀Au₂O₂

Rocchigiani, Luca Fernandez-Cestau, Julio Chambrier, Isabelle Hrobárik, Peter Bochmann, Manfred

Journal of the American Chemical Society (2018) 140, 26 8287-8302

a=14.6204(2)Å b=5.96800(10)Å c=19.8075(2)Å

α=90° β=98.1470(10)° γ=90°

C₃₁H₃₈AuNO₂

Chambrier, Isabelle Roşca, Dragoş-Adrian Fernandez-Cestau, Julio Hughes, David L.Budzelaar, Peter H. M.Bochmann, Manfred

Organometallics (2017) 36, 7 1358-1364

a=28.8593(4)Å b=12.2845(2)Å c=33.8899(5)Å

α=90° β=104.6810(10)° γ=90°

C_199.40H_202.20Au₈N_8,0.6(C)

Roşca, Dragoş-Adrian Bochmann, Manfred

Organometallics (2015) 35, 1 27

a=26.9936(10)Å b=26.9936(10)Å c=12.952(5)Å

α=90.00° β=90.00° γ=90.00°

C₅₀H₅₄Au₂N_2,2(C₆H₆)

Roşca, Dragoş-Adrian Bochmann, Manfred

Organometallics (2015) 35, 1 27

a=12.609(2)Å b=26.9775(15)Å c=17.476(2)Å

α=90.00° β=121.135(8)° γ=90.00°

Compound 6.3(C6H6)

C₅₄H₇₂AUN_4,C₂₉H₄₃O_2,3(C₆H₆)

Roşca, Dragoş-Adrian Fernandez-Cestau, Julio Hughes, David L.Bochmann, Manfred

Organometallics (2015) 34, 11 2098-2101

a=15.1887(11)Å b=24.4609(17)Å c=24.3362(17)Å

α=90° β=94.2705(11)° γ=90°

Compound 4.C6H6

C₅₄H₇₂Au₂N₄O_2,C₆H₆

Roşca, Dragoş-Adrian Fernandez-Cestau, Julio Hughes, David L.Bochmann, Manfred

Organometallics (2015) 34, 11 2098-2101

a=15.3438(11)Å b=19.5250(14)Å c=19.6769(14)Å

α=90° β=92.122(5)° γ=90°

Compound 5.3(THF)

C₈₂H₁₀₈AU₃N₆O_3,3(C₄H₈O)_,OH

Roşca, Dragoş-Adrian Fernandez-Cestau, Julio Hughes, David L.Bochmann, Manfred

Organometallics (2015) 34, 11 2098-2101

a=12.4797(9)Å b=41.783(3)Å c=21.4315(15)Å

α=90° β=94.2010(10)° γ=90°